陈勇,陈月,邱长军,樊湘芳.CeO2纳米杆的制备与表征[J].南华大学学报(自然科学版),2015,29(2):63~65, 83.[CHEN Yong,CHEN Yue,QIU Chang-jun,FAN Xiang-fang.Synthesis and Characterization of CeO2 Nano-rods[J].Journal of University of South China(Science and Technology),2015,29(2):63~65, 83.] |
CeO2纳米杆的制备与表征 |
Synthesis and Characterization of CeO2 Nano-rods |
投稿时间:2014-10-16 |
DOI: |
中文关键词: 低温水热法 氧化铈 纳米杆 抗紫外线 |
英文关键词:low-temperature hydrothermal process CeO2 nano-rods UV-shielding |
基金项目:南华大学博士启动基金资助项目(2013XQD01);湖南省教育厅优秀青年项目(14B152);湖南省重点学科建设基金资助项目(湘教发[2011]76号);湖南省高校科技创新团队支持计划基金资助项目(湘教通[2012]318号);湖南省高校重点实验室基金资助项目(湘财教指[2014]85号) |
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中文摘要: |
在低温水热条件下,通过一步法合成二氧化铈纳米杆.采用XRD、SEM和TEM对合成的样品进行表征,并利用紫外线可见光谱仪对氧化铈纳米杆的抗紫外线能力进行检测.实验结果表明:用醋酸铈和磷酸氢钠制备的氧化铈纳米杆形貌比较细长,平均直径~10 nm,平均长度~400 nm,且生长方向沿着<112>方向生长;另外,氧化铈纳米杆有很宽的吸收波段和很强的吸收能力,可作为理想的紫外线屏蔽材料. |
英文摘要: |
CeO2 nano-rods are synthesized by the facile and efficient hydrothermal process in this experiment.The synthesized samples are characterized by using XRD,SEM and TEM,and the UV-shielding properties of CeO2 nano-rods are examined with an UV-vis spectrophotometer.The results show that morphology of the nano-rods synthesized by cerium acetate and sodium hydrogen phosphate is relatively slender,with an average diameter of ~ 10 nm,the average length of ~ 400 nm,and the growth direction is along the <112> direction.In addition,CeO2 nano-rods have a very broad absorption band and strong absorption capacity,so it can act as an efficient UV-shielding candidate. |
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